Quartz Crystal Microbalance QCM

Quartz Crystal Microbalance for in situ flux calibration; positioning directly under the substrate for accurate rate measurements
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  • Quartz Crystal Microbalance for thin-film measurements
  • Compatible with most oscillator devices
  • Mounting Flange DN40CF (2.75” O.D.), rotatable
  • Linear travel 150 mm, 200 mm or 250 mm
  • Bakeable up to 250°C

Introduction

This standard Quartz Crystal Microbalance can be used for in situ flux calibration in many MBE applications. Due to the linear travel it is possible to move the quartz directly under the substrate for accurate rate measurements.

The main component is a gold-plated piezo crystal which oscillates with its natural frequency. If material hits the quartz surface and sticks there the mass of the quartz will change. The change of mass results in a change of the natural frequency which will be detected.

The QCM instrument enables the measurement of thickness changes in the range of sub atom layers, i.e. < 1 nm. To overcome disturbing temperature effects the QCM is water-cooled.

QCM detail
QCM oscillator head with sight of gold-plated piezo crystal

Application

Typical applications for the QCM Quartz Crystal Microbalance are:

  •   Flux calibration of effusion cells with regard to the cell temperature

  •   Uniformity measurements using the linear travel to measure the flux rate at different positions

  •   In-situ thickness control during the MBE process

Technical Data

Mounting FlangeDN40CF (O.D. 2.75")
In‑vacuum dimensions100...500 mm, others on request
Airside dimensions311...726 mm (depending on linear travel length)
Electrical feed-throughBNC (to oscillator)
Bakeout temperatureup to 250 °C
Cooling / water cooling2 x Swagelok Ø 8 mm
Extended length Edepending on linear travel length
Measurement rangedepends on oscillator device

Specific Data

For general information on CF mounting flanges see Flange and Gasketdimensions.
ProductFlange [CF]Linear travel
[mm]
UHV dimensions
[mm] specify L with order
QCM40150LxxxD35
Power graph
QCM40200LxxxD35
Power graph
QCM40250LxxxD35
Power graph
QCM40300LxxxD35
Power graph
QCM40400LxxxD35
Power graph

Example: QCM 40-200-L100D35 is a Quartz Crystal Microbalance on DN40CF-flange with 200 mm shift, integrated water-cooling, retracted in-vacuum length L = 100 mm and extended length T+L = 300 mm. The center of the active quartz surface is located at T+L-13 mm = 287 mm. The surrounding tube has to have an inner diameter ≥35 mm.